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Edexcel A Level Chemistry: 15: Transition Metals

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This flashcard set introduces transition metals, explaining their position in the periodic table, defining characteristics, and exceptions such as scandium and zinc. It also includes the electron capacity of the d orbital.

Where are transition metals found in the periodic table?

D block

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Key Terms

Term
Definition

Where are transition metals found in the periodic table?

D block

What are transition metals?

D block elements that can form one or more stable ions with incompletely filled d-orbitals

Which d block period 4 elements are not transition metals?

Scandium and Zinc

How many electrons can the d orbital hold?

10

When ions are formed, which electrons are removed first?

The s electrons


Why is Scandium not a transition metal?

It only forms one ion, Sc3+, which has an empty d subshell


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TermDefinition

Where are transition metals found in the periodic table?

D block

What are transition metals?

D block elements that can form one or more stable ions with incompletely filled d-orbitals

Which d block period 4 elements are not transition metals?

Scandium and Zinc

How many electrons can the d orbital hold?

10

When ions are formed, which electrons are removed first?

The s electrons


Why is Scandium not a transition metal?

It only forms one ion, Sc3+, which has an empty d subshell


Why is zinc not a transition metal?

It only forms one ion, Zn2+, which has a full d subshell

How many stable oxidation states does Vanadium have?

4

What are the stable oxidation states of Vanadium?

II, III, IV, V

What do transition metals have?

Variable oxidation states

What conditions must be met to form a compound of complex with an ion of a certain oxidation number?

The energy given out when the ion forms a compound or complex needs to be greater than the ionisation energy

How do transition metals form ions?

By loosing electrons from their 4s and 3d subshells

When does the energy released when an ion forms a complex or compound increase?

When the ionic charge increases.

What are complex ions?

Metal ions surrounded by datively covalently bonded ligands

What is a ligand?

An atom, ion or molecule which donates a pair of electrons to a central metal atom or ion.


What are monodentate ligands?

Ligands with one lone pair

What are bidentate ligands?

Ligands with two lone pairs


What are multidentate ligands?

Ligands with more than two lone pairs


What are examples of monodentate ligands?

H2O, NH3, Cl-

What is an example of a multidentate ligands?

EDTA 4-

What is the name for water in a complex?

Aqua

What is the name for a hydroide group in a complex?

hydroxo

What is the name for ammonia in a complex?

Ammine

What is the name for chloride in a complex?

Chloro

How many colours traditionally make up white light?

7

Why are transition metal complexes coloured?

Electrons split into two energy levels when ligands attach. If an electron absorbs light, it can move to a higher energy level, and the light reflected is the colour seen

With 6 ligands, what shape is a complex?

Octahedral

With 4 ligands, what shape is a complex?

Tetrahedral or square planar

With 2 ligands, what shape is a complex?

Linear

What is an example of a linear complex?

Tollen's reagent

What is cis-platin?

An anti-cancer drug which has a square planar shape

What does a cis- prefix indicate?

That the identical ligands are next to each other

What does a trans- prefix indicate?

That the identical ligands are opposite each other

How does cis-platin kill cancer cells?

It forms a bond between the two strands of DNA which prevents them from separating, and therefore prevents replication

How is trans-platin different to cis-platin?

It is toxic and much less effective at targeting cancer

Why does reducing the number of ligands increase stability?

The system becomes more disordered and there is an increase in ∆S system

What causes the greatest increase in stability?

Exchanging a monodentate ligand for a multidentate ligand

How is Fe held in haemoglobin?

By forming dative bonds with four nitrogens in the structure, in a square planar


What else is bonded to the Fe in haemoglobin?

Globin (a protein) and Oxygen

Why is carbon monoxide poisonous?

Because the dative bond between carbon monoxide and haemoglobin is stronger than with oxygen, so any CO breathed in will bins with the haemoglobin and not break easily

What is the equation for the reaction between aqueous NaOH and copper(II) sulfate solution?

[Cu(H2O)6]2+ + 2OH- ---> [Cu(H2O)4(OH)2] + H2O

What colour is [Cu(H2O)4(OH)2]?

Blue precipitate

What is the equation for the reaction between aqueous ammonia and copper (II) sulfate?

[Cu(H2O)6]2+ + NH3 ----> [Cu(H2O)4(OH)2] + 2NH4+


What is the equation for the reaction between the blue copper precipitate and aqueous ammonia?

[Cu(H2O)4(OH)2] + 4NH3 ----> [Cu(NH3)4(H2O)2]2+ + 2H2O + 2OH-

What colour is [Cu(NH3)4(H2O)2]2+?

Deep blue solution

What is the equation for the reaction between copper (II) sulfate solution and conc HCl?

{CU(H2O)6]2+ + 4Cl ----> [CuCl4]2- + 6H2O

What is the colour change when hydrochloric acid is added to copper sulfate solution?

Blue to green to yellow

What is the equation for the reaction between hexaaquacobalt(II) and aqueous sodium hydroxide?

[Co(H2O)6]2+ + 2OH- ----> [Co(H2O)4(OH)2] + 2H2O

What is the colour change when sodium hydroxide is added to hexaaquacobalt(II)?

Pink solution to blue precipitate

How many reactions occur between hexaaquacobalt(II) and ammonia?

2

What is the acid-base reaction between hexaaquacobalt(II) and NH3?

[Co(H2O)6]2+ + 2NH3 ----> [Co(H2O)4(OH)2] + 2NH4+

What is the equation for the reaction between [Co(H2O)4(OH)2] and NH3?

[Co(H2O)4(OH)2] + 6NH3 ----> [Co(NH3)6]2+ + 4H2O + 2OH-

What is the colour change between hexaaquacobalt(II) and ammonia?

Precipitate dissolves to a brown solution

What is the colour od the [Co(NH3)6]3+ ion?

Yellow

What is the equation for the reaction between hexaaquacobalt(II) and conc HCl?

[Co(H2O)6]2+ + 4Cl- ----> [CoCl4]2- + 6H2O

What is the colour change when conc HCl is added to the hexaaquacobalt (II) solution?

Pink to blue

What is the equation for the reaction between hexaaquairon(II) and sodium hydroxide?

[Fe(H2O)6]2+ + 2OH- ----> [Fe(H2O)4(OH)2] + 2H2O

What is the colour change in the reaction between hexaaquairon(II) and sodium hydroxide?

Pale green solution forms a green precipitate

What is the equation for the reaction between hexaaquairon(II) and NH3?

[Fe(H2O)6]2+ + 2NH3 ----> [Fe(H2O)4(OH)2] + 2NH4+

What is the equation for the reaction between hexaaquairon(III) and sodium hydroxide?

[Fe(H2O)6]3+ + 3OH- ----> [Fe(H2O)3(OH)3] + 3H2O

What is the colour change for the reaction between hexaaquairon(III) and sodium hydroxide?

Yellow-brown solution forms and brown precipitate

What is the equation for the reaction between hexaaquairon(III) and NH3?

[Fe(H2O)6] + 3NH3 ----> [Fe(H2O)3(OH)3] + 3NH4

What are the colours shown by chromium compounds affected by?

Some compounds have different colours as solids and aqueous solutions
The colour of the solution depends on the concentration
The presence of dissolved oxygen in an aqueous solution can affect the colour seen

What is the equation for the reaction between the hexaaquachromium(III) ion and aqueous sodium hydroxide?

[Cr(H2O)6]3+ + 3OH- ----> [Cr(H2O)3(OH)3] + 3H2O

What is the colour change for the reaction between hexaaquachromium(III) and sodium hydroxide?

Green or violet solutions forms a green precipitate

What is the equation for the reaction between hexaaquachromium(III) and NH3?

[Cr(H2O)6]3+ + 3NH3 ----> [Cr(H2O)3(OH)3] + 3NH4+

What happens to the precipitate [Cr(H2O)3(OH)3] when it is dissolved?

It dissolves to form a green solution of [Cr(H2O)2(OH)4]-

What happens to the precipitate [Cr(H2O)3(OH)3] when excess ammonia is added?

It is slow to dissolve but eventually a violet or purple solution of [Cr(NH3)6]3+ forms

What is the equation for the reaction between [Cr(OH)6]3- and hydrogen peroxide?

2[Cr(OH)6]3- + 3H2O2 ----> 2CrO42- + 2OH- + 8H2O

What is the colour change for the reaction between the chromium complex and hydrogen peroxide?

Green solution to yellow solution

What is hydrogen peroxide?

An oxidising agent

How does the chromate ion change with acidity?

In alkaline solution, the chromate(VI) ions are stable, but in acidic solution the dichromate(VI) are most stable

What colour change is seen if acid is added to chromate ions?

Yellow to orange

What can dichromate(VI) ions be reduced by?

Zinc

What is the equation for the reduction of dichromate ions using zinc?

Cr2O72- + 14H+ +3Zn ----> 2Cr3+ + 7H2O + 3Zn2+

What is the colour change when dichromate ions are reduced?

Orange to green

What is the colour change when Cr3+ is reduced to Cr2+?

Green to blue

What reaction happens when NaOH is added to [Cr(H2O)3(OH)3]?

It forms [Cr(OH)6]3-

What colour are V2+ ions?

Purple

What colour are V3+ ions?

Green

What colour are (VO)2+ ions?

Blue

What colour are (VO2)+ ions?

Yellow

In what compound does vanadium have a +4 oxidation number?

(VO)2+

In what compound does vanadium have a +5 oxidation number?

(VO2)+

Why is it easy to demonstrate a change in oxidation number with vanadium?

Because its colour changes are so distinctive

What can be used to reduce vanadium from +5 to +2?

Zinc

What is the equation for the reduction of vanadium from +5 to +4?

2(VO2)+ + 4H+ + Zn ----> 2(VO)2+ + Zn2+ + 2H2O

What is the equation for the reduction of vanadium from +4 to +3?

2(VO)2+ + 4H+ + Zn ----> 2V3+ + Zn2+ + 2H2O

What is the equation for the reduction of vanadium from +3 to +2?

2V3+ + Zn ----> 2V2+ + Zn2+

What is the equation for the reduction of vanadium from +2 to 0?

2V2+ + Zn ----> 2V + Zn2+

Which of the vanadium reductions is not thermodynamically feasible?

+2 to 0

In what state are transition metals usually used as catalysts?

Solid, as a powder

What is the catalyst in the contact process?

V2O5 - Vanadium Pentoxide

What are the steps of surface adsorption theory?

Adsorption
Reaction
Desorption

What is adsorption?

One or more reactants become attached to the catalyst

What is the reaction step in surface adsorption theory?

Following the weakening of the bonds in the adsorbed reactants

What is desorption?

The reaction product becomes detached from the surface of the catalyst

What are the reactions that occur on the surface of vanadium in the contact process?

V2O5 + SO2 ----> V2O4 + SO3

| V2O4 + 0.5O2 ----> V2O5

What are the problems tackled by catalytic converters?

Increased pollution levels
Carbon monoxide emissions
Nitrogen monoxide emissions

What are the transition metals used in catalytic converters?

Platinum and rhodium, sometimes palladium

What is the equation for the reaction between Carbon monoxide and nitrogen monoxide?

2CO + 2NO ----> 2CO2 + N2

Why does the reaction between CO and NO occur on catalytic converters?

Because the molecules of CO and NO are adsorbed and then, because their bonds are weakened, they react together to form CO2 and N2, which are then desorbed

What is a key feature of homogeneous catalysts?

The formation of an intermediate species for which a specific formula can be written

What is the equation for the reaction between persulfate ions and iodide ions?

S2O82- + 2I- ----> 2SO42- + I2

What is the catalyst in the reaction between iodide and persulfate ions?

Fe2+

What are the steps in the reaction between I- and S2O82-?

S2O82- and 2Fe2+ react together to form 2SO42- and 2Fe3+

| 2Fe3+ react with 2I- to form 2Fe2+ and I2

Why do the Fe2+ and S2O82- react together?

Because they do not repel each other, as they have the opposite charge

What is the alternative mechanism for the reaction between I- and S2O82-?

2Fe3+ + 2I- ----> 2Fe2+ + I2

| S2O82- + 2Fe2+ ----> 2SO42- + 2Fe3+