Solution Manual for Separation Process Engineering: Includes Mass Transfer Analysis, 4th Edition

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SOLUTION MANUAL
for
SEPARATION PROCESS ENGINEERING
4 th Edition
by
Phillip C. Wankat

3
TABLE OF CONTENTS
SAMPLE: Course Syllabus in Separation Process Engineering p. 4
EXAMPLE Schedule A: Equilibrium Staged Plus Membranes with Computer Labs p. 9
EXAMPLE Schedule B: Classical Equilibrium Staged Course with Computer Lab p. 10
EXAMPLE Schedule C: Vapor-Liquid Separations Course with Computer Lab p.11
EXAMPLE Schedule D: Equilibrium Staged Separations Plus Adsorption, Ion Exchange &
Chromatography with Computer Lab* p. 12
*Assumes students know Fickian Diffusion & Mass Transfer
EXAMPLE Schedule E: Classical Equilibrium Stage Course Without Computer Lab p. 13
EXAMPLE Schedule F: Mass Transfer & Diffusion Plus Mass Transfer Analysis of Distillation,
Absorption, Membrane & Sorption Separations* p.14
*Assumes students have had an Equilibrium-Staged Separations Course
EXAMPLE Schedule G. Separations Overview Course – Distillation, Absorption,
Crystallization, Membrane Separation, Adsorption, and Chromatography. p.15
SOLUTIONS TO PROBLEMS:
Chapter 1 p. 17
Chapter 2 p. 18
Chapter 3 p. 53
Chapter 4 p. 66
Chapter 5 p. 112
Chapter 6 p. 135
Chapter 7 p. 147
Chapter 8 p. 170
Chapter 9 p. 217
Chapter 10 p. 255
Chapter 11 p. 282
Chapter 12 p. 293
Chapter 13 p. 324
Chapter 14 p. 368
Chapter 15 p. 390
Chapter 16 p. 405
Chapter 17 p. 427
Chapter 18 p. 440
Chapter 19 p. 480

4
SAMPLE COURSE SYLLABUS*
CHE 306 DESIGN SEPARATION PROCESSES
INSTRUCTOR: Professor Phillip C. Wankat
Office: FRNY 2037C
E-mail: wankat@purdue.edu (I usually answer quickly between 8 am and
5:30 pm. Use e-mail to communicate with Prof. Wankat for help.)
Office Hours: MWF 10:30-11:50 A.M. These times are reserved for 306 students.
On Wednesdays I will be in the computer lab from 1:30 to 3:20 P.M.
Other times by appointment only.
TA's – Office hours will be M 2:30 to 3:30, T 1:00 to 3:00 and W 1:00 to 2:30 in FRNY B142A
(starting second week of semester).
Prerequisites: Must have passed Mass & Energy Balances and Thermodynamics
TEXTBOOK: P.C. Wankat, Separation Process Engineering, 4th edition Prentice Hall, 2016.
Goals*: By the end of CHE 306 you should be able to:
1. Design flash distillation by hand and computer calculations;
2. Design distillation systems by hand and computer calculations;
3. Design extraction systems by hand and computer calculations;
4. Design membrane separation systems.
Importance: Separations constitute 50 to 90% of the cost (capital and operating) of chemical
plants. Distillation is the most important separation method in the chemical and petroleum
industries. Separations are one of the key items which delineate chemical engineering from the
other engineering disciplines.
Course The basic course outline* is:
Structure: 1. Introductory Material (1 week)
2. Flash Distillation (1 week)
3. Binary Distillation (2 weeks)
4. Multicomponent Distillation (2 weeks)
5. Complex Distillation (2 weeks)
6. Batch Distillation (1 week)
7. Distillation Design (1 week)
8. Absorption, Stripping, & Extraction (2 weeks)
9. Extraction (1 week)
10. Membrane separations (2 weeks)
The detailed course outline is attached. The typical weekly schedule will be:
Monday, Wednesday and Friday: 2 Lectures plus optional help.
Wednesday/Thursday: Computer Lab when scheduled
Since the schedule will sometimes deviate from this pattern, follow your detailed course outline.

5
Suggested Read book before class. Come to class prepared. There will be
Study short quizzes to encourage preparation. New material
Procedure: will be presented in class as needed. Material in the book that is a review
or is easy to understand will not be lectured on. Ask questions if the book
is not clear. After class, reread the book. Make extensive notes on or in
the book. Before each exam summarize your notes on one page, and then
reduce to 3x5 card (double-sided) you can take into the exam.
The suggested way to do homework: First, work on all problems by
yourself. Then, meet with your study group to check answers and to
complete solution of more difficult problems. Ask for help once these
other efforts have failed. Finally, prepare your own solution to hand in if
the homework will be graded. It is important to solve a lot of problems
including homework that is not handed in.
You should spend 9 to 12 hours (including class & lab time) on this course
every week. If you are spending less, work more problems both
individually and in your study group.
Quizzes*: To encourage students to prepare for and attend class, there will be a series
of 10 short quizzes, which are 9% of the course grade. The lowest grade
will not count, which is equivalent to one free absence. After that an
absence will be a zero. Students who turn in a quiz with their name on it
and who stay the entire period and pay attention will automatically earn
50%. There will be no quiz make-ups and no taking quizzes late (Part of
the 50% for attendance is being on time – if you want this credit make
attendance a high priority. In other words, an interview at Purdue is NOT
a valid excuse for missing a quiz.) Missing 2 quizzes for plant trips will
cost 1% of the course grade – a small penalty. Writing another student’s
name on a quiz and turning it in for a grade will be treated as a form of
cheating. Graded quizzes will be passed out in labs or will be available
from Karen Heide in FRNY 1029.
Homework*: There will be 8 homework assignments which are handed in. Students
who solve all of the problems are very likely to see their efforts rewarded
by higher test scores. The homework that is handed in will be 6% of the
course grade. The professor and TAs will grade one problem selected by
the professor and one problem selected by the student – write the problem
you want graded on the top of the assignment. Graded homework
assignments will be passed out in labs or will be available from Karen
Heide in FRNY 1029. Work in groups on homework is encouraged. Turn
in your own solution (not Xerox copy), but please list names of group
members on it.
Exams*: Arrange your schedule to be available for the night exams on Sept. 30 and
Nov. 4. The third exam, which is not a cumulative final exam, will be
during finals. Exams (including the lab test) are 70% of the course grade.
Your lowest exam will be 10% and the other three exams will count as
20% each. Exams (except the lab test) are closed book, but students will

6
be allowed and encouraged to have one 3 x 5 card (double-sided) with
information on it. All electronic devices (other than a calculator) must be
turned off and be buried in your back pack. Use of these devices will be
considered to be cheating. Graded exams will be passed out in labs or will
be available from Karen Heide in FRNY 1029.
DO NOT MAKE TRAVEL PLANS UNTIL YOU KNOW THE FINALS SCHEDULE
Make-Up Exam*: Students are strongly urged to make attendance at exams a very high
personal priority and make appropriate arrangements to be present at all
exams. If an exam is missed students may choose to make it their lowest
exam grade and receive a zero for 10% of their course grade.
Alternatively, a single comprehensive make-up exam (available only for
students who miss a test) will be administered during finals period (after
Exam 3). This will be the only make-up exam available. In cases of
extreme duress (e.g., hospitalization) talk to Prof. Wankat for other
arrangements.
Computer Lab*: Computer labs are scheduled for Wednesdays and Thursdays in FRNY
1022. If you want to switch lab sections see the undergraduate secretary
during the first week of classes to see if this is possible. Work in lab will
initially be done individually and later in the semester in assigned 3- or 4-
person groups. Feel free to help other students and to ask for help during
lab. Laboratory will use the ASPEN Plus simulation package. Most of the
lab assignments are in your textbook; thus, you will need to bring your
textbook to lab.
The laboratory (not including the lab test) will be 15% of the course grade.
Attendance & attention in computer lab is required, and will be 6% of the
course grade. There will be a limited opportunity to do lab in advance or
make-up a missed laboratory, but without help from the TA (arrange with
your TA to show you have done the lab work). Because seating is limited,
students must attend their scheduled laboratory period unless arrangements
are made in advance to attend a lab session that has open seats. Group lab
reports are required for two labs. Lab groups are expected to help each
other for the two labs that require lab reports. Only questions from the
entire group will be answered by the TA or professor for laboratory help.
Lab reports will be limited to two pages of text plus one page of figures
and tables. The two lab reports and the mastery lab quiz each count 3.0%
of the course grade.
There will be a lab test worth 20% of course grade in FRNY 1022 on
November 12th and 13 th during your regularly scheduled lab hours. Work
will be done individually. The lab test will be open book and open notes.
The use of e-mail, the Internet, or old computer files will not be allowed
during the lab test. Plan on being present.

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7
Summary Quizzes 9% (1/2 attendance & attention)
of Grading*: Graded Homework 6%
Exam 1 to 3 plus lab test 70% (lowest grade is 10% others are 20%
each).
Lab Grade (attendance, lab reports & lab quiz) 15% (6% attendance)
Extra Credit 0%
Grading Scale*: Guaranteed Grade Scale for +/- scale:
Grade GPA Value Recommended Range
A+,A 4.0 93‐100
A‐ 3.7 90.0 ‐ 92.9
B+ 3.3 87.0 ‐ 89.9
B 3.0 83.0 ‐ 86.9
B‐ 2.7 80.0 ‐ 82.9
C+ 2.3 77.0 ‐ 79.9
C 2.0 73.0 – 76.9
C‐ 1.7 70.0 – 72.9
D+ 1.3 67.0 – 69.9
D 1.0 63.0 – 66.9
D‐ 0.7 – becomes
lowest passing
grade
60.0 – 62.9
F 0.0 < 60.0
Slightly lower cut off scores may be used at the discretion of the instructor.
Lectures: According to University regulations, it is the responsibility of students to
attend all class sessions and to make up any material that is missed. To
aid students, a TA will take notes of every lecture. These notes will be
placed on Blackboard. Note: there is abundant evidence that students who
regularly attend lectures tend to earn higher grades.
Optional Help The Professor or a TA will hold a help session during the regularly
scheduled class (9:30 to 10:20 a.m. in FRNY G140) one day most weeks
on Monday, Wednesday or Friday (see detailed course outline). The
Wednesday class on the day of the two night exams will be an optional
help session. Additional help sessions can be arranged before tests if
students request them. In addition the professor and the TAs will have
office hours that you are strongly encouraged to use. Since office hours
are traditionally not heavily used early in the semester, this is a good time
to get into the habit of attending office hours. Also, feel free to discuss
questions with your laboratory instructor during laboratory.

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Feedback to With a large class it is essentially impossible for a professor to know
Prof. Wankat each student and to be aware of the difficulties they are having in learning
the course material. To provide feedback to Prof. Wankat a group of
student representatives will be constituted with one representative from
each laboratory section. This group will meet with Prof. Wankat once per
week to provide anonymous feedback from all the students in the course.
Professional Students in CHE 306 are continuing on a program of study to become
Behavior: chemical engineers. Engineers are expected to uphold the code of ethics,
which includes "Being Honest," "Engineers shall build their professional
reputations on the merits of their services," and "Engineers shall act in
such a manner as to uphold and enhance the honor, integrity, and dignity
of the engineering profession." Students in CHE 306 will be expected to
behave in an ethical and professional manner, which includes:
1. Honesty on quizzes, exams, and lab test. Cell phones, pagers, personal
computers, MP3 players, personal digital assistants, & similar
electronic devices must be off and not in sight – no phone calls, text
messaging or use of storage available in the electronic device.
Alphanumerical data or programs are not allowed in calculators. The
use of head phones is not allowed. Note: since you will be allowed the
use of a 3x5 card, there is no reason to try and beat the system.
2. No plagiarism or copying.
3. Claim credit for homework/laboratory only if you were involved in the
solution. [Do NOT turn in a copy that you do not understand.] This is
common sense – not cheating. Students who copy homework (strictly
speaking this is legal, but stupid) will do poorly on exams and receive
low grades because of this.
4. No disruption of class. Because cell phones are disruptive, please turn
cell phones off before lectures or lab. In addition, since many students
report that when students talk to neighbors during lecture it is
disruptive, please do not do it.
5. Make a concerted, diligent effort to learn.
The following are OK in lab if done in a way that does not disturb other students:
1. Drinking water (no soft drinks in lab as they really mess up key boards if spilled).
2. Very modest amount of eating of snacks.
3. Taking a break – if you need a coke drink it outside the lab. If you need to smoke, take a
break outside of the building. Do your texting on break also.
4. Asking another student for help on the computer assignment.

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EXAMPLE Schedule B: Classical Equilibrium Staged Course
Skip Chapters 15-19 in 4th edition
Class Subject Reading:
1 Introduction. Phase Equilibrium Chapt. 1
2 Phase Equilibrium, Start Flash Chapt. 2
3 Flash – Binary & Multicomponent Chapt. 2
4 Flash – Binary & Multicomponent Chapt. 2
5 Lab 1 Intro to Aspen Plus. Lab 1, App. C2
6 Flash – MultiComponent and Aspen Plus Chapt. 2
7 Binary Distillation Chapt. 3
8 Lab 2 – Flash Distillation. Lab 2, App C2
9 McCabe-Thiele Chapt. 4
10 McCabe-Thiele Chapt. 4
11 Lab 3– Binary Distillation. Lab 3, App C4
12 McCabe-Thiele
13 Profiles & Intro. M. C. Distillation Chapt. 5
14 Lab 4 – M. C. Distillation. Lab 4, App C6
15 EXAM #1.
16 Review Test & M. C. Dist. Mass Balances Chapt. 5
17 Lab 5 - M.C. Distillation. Lab 5, App C6
18 M. C. Distillation Chapt. 6
19 Short Cut Distillation Chapt. 7
20 Lab 6 – Complex Distillation, Lab 7, App C8
21 Complex Distillation

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11
EXAMPLE Schedule C: Vapor-Liquid Separations Course
Skip Chapters 13, 14, part 16, 17-19 in 4 th edition
Class Subject Reading:
1 Introduction. Phase Equilibrium Chapt. 1
2 Phase Equilibrium, Start Flash Chapt. 2
3 Flash – Binary & Multicomponent Chapt. 2
4 Flash – Binary & Multicomponent Chapt. 2
5 Lab 1 Intro to Aspen Plus. Lab 1, App. C2
6 Flash – MultiComponent and Aspen Plus Chapt. 2
7 Binary Distillation Chapt. 3
8 Lab 2 – Flash Distillation. Lab 2, App C2
9 McCabe-Thiele Chapt. 4
10 McCabe-Thiele Chapt. 4
11 Lab 3– Binary Distillation. Lab 3, App C4
12 McCabe-Thiele
13 Profiles & Intro. M. C. Distillation Chapt. 5
14 Lab 4 – M. C. Distillation. Lab 4, App C6
15 EXAM #1.
16 Review Test & M. C. Dist. Mass Balances Chapt. 5
17 Lab 5 - M.C. Distillation. Lab 5, App C6
18 M. C. Distillation Chapt. 6
19 Short Cut Distillation Chapt. 7
20 Lab 6 – Complex Distillation, Lab 7, App C8
21 Complex Distillation

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